Sodium Bicarbonate → HCID 22760515, compound

HRID 1703861Notes

Reaction equation

HRID 1703861 reaction equation
Br.[Cl:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2([OH:22])[CH2:13][S:12][C:11](=[N:14][CH2:15][CH:16]3[CH2:20][CH2:19][CH2:18][CH2:17]3)[N:10]2[CH3:21])=[CH:5][C:4]=1[S:23](=[O:26])(=[O:25])[NH2:24].C(=O)(O)[O-].[Na+]>>[Cl:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2([OH:22])[CH2:13][S:12][C:11](=[N:14][CH2:15][CH:16]3[CH2:20][CH2:19][CH2:18][CH2:17]3)[N:10]2[CH3:21])=[CH:5][C:4]=1[S:23](=[O:25])(=[O:26])[NH2:24]

Participants

3

Reactant 2

HCID 516892Sodium BicarbonateHCID 22760571HCID 22760571, compound

Product 1

HCID 22760515HCID 22760515, compound

Procedure

6 g of 4-(4-chloro-3-sulfamoylphenyl)-2-cyclopentylmethylimino-3-methyl-1,3-thiazolidine-4-ol-hydrobromide were reacted according to the prescription given in Example 2(c) with sodium bicarbonate. Colorless solid body: decomposition beginning at 115° C. γC=N 1615 cm-1.

Workup

  1. custombeginning at 115° C.

Sources & evidence

ORD record
ord-d612691ffdeb4652b4a5a72df1ffbf71
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

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