HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-Diethylthiourea → 3-Ethyl-2-ethylimino-4-(4-bromo-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-Diethylthiourea | HCID 2735009 | — |
| Reactant | 4'-Bromo-3'-sulfamoyl-2-chloroacetophenone | HCID 22760605 | — |
| Product | 3-Ethyl-2-ethylimino-4-(4-bromo-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride | HCID 22760569 | — |
Reaction Steps
4.6 g of 4'-bromo-3'-sulfamoyl-2-chloroacetophenone and 1.8 g of ground 1,3-diethylthiourea were reacted and worked up according to the prescription given in Example 12. Colorless solid body, decomposition beginning at 103° C., C=N 1615 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125614 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-92285eb56dfc49749d4e9385e2fc9f71 |
| Source note | uspto-grants-1978_11 |