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Hydrochloric Acid → 2-Chloro-4'-methyl-3'-sulfamoylacetophenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Isopropanol | HCID 3776 | — |
| 反応物 | 4'-Methyl-3'-sulfamoyl-diazoacetophenone | HCID 54047535 | — |
| 溶媒 | Diglyme | HCID 8150 | — |
| 生成物 | 2-Chloro-4'-methyl-3'-sulfamoylacetophenone | HCID 13628783 | — |
反応手順
10 g of 4'-methyl-3'-sulfamoyl-diazoacetophenone were reacted as prescribed in Example 66(b) in diethylene glycol dimethyl ether with 37% HCl and worked up. Colorless crystals, melting point: 166° C. (from isopropanol).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04125614 |
| 出典データセット | uspto-grants-1978_11 |
| ORD ID | ord-24bba5bebc2f4a6a809fa02fdd801380 |
| 出典メモ | uspto-grants-1978_11 |