Cyclooctylamine → HCID 22760619, compound

HRID 1703909Notes

Reaction equation

HRID 1703909 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][C:3]=1[S:11](Cl)(=[O:13])=[O:12].[CH:15]1([NH2:23])[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16]1>>[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][C:3]=1[S:11](=[O:13])(=[O:12])[NH:23][CH:15]1[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16]1

Participants

3

Reactant 2

HCID 2903CyclooctylamineHCID 756134-Chloro-3-(chlorosulphonyl)benzoic acid

Product 1

HCID 22760619HCID 22760619, compound

Procedure

25.5 g of 4-chloro-3-chlorosulfonylbenzoic acid were reacted as prescribed in Example 75(a) with 45 g of cyclooctyl amine and worked up. The crystallized 4-chloro-3-cyclooctylsulfamoylbenzoic acid so obtained was dried end reacted without further purification in thionyl chloride as prescribed in Example 74(a). Colorless crystals, melting point: 134° C.

Sources & evidence

ORD record
ord-5dfcd263e2f7457e984c106b868c3a0c
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

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