HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclooctylamine → HCID 22760619, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclooctylamine | HCID 2903 | — |
| Reactant | 4-Chloro-3-(chlorosulphonyl)benzoic acid | HCID 75613 | — |
| Product | HCID 22760619 | HCID 22760619 | — |
Reaction Steps
25.5 g of 4-chloro-3-chlorosulfonylbenzoic acid were reacted as prescribed in Example 75(a) with 45 g of cyclooctyl amine and worked up. The crystallized 4-chloro-3-cyclooctylsulfamoylbenzoic acid so obtained was dried end reacted without further purification in thionyl chloride as prescribed in Example 74(a). Colorless crystals, melting point: 134° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125614 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-5dfcd263e2f7457e984c106b868c3a0c |
| Source note | uspto-grants-1978_11 |