Hydrochloric Acid → HCID 22760665, compound

HRID 1703914Notes

Reaction equation

HRID 1703914 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2([OH:16])[CH2:12][S:11][C:10](=[N:13][CH3:14])[N:9]2[CH3:15])=[CH:4][C:3]=1[S:17](=[O:28])(=[O:27])[NH:18][CH2:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][C:21]=1[Cl:26].Cl>>[ClH:1].[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2([OH:16])[CH2:12][S:11][C:10](=[N:13][CH3:14])[N:9]2[CH3:15])=[CH:4][C:3]=1[S:17](=[O:28])(=[O:27])[NH:18][CH2:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][C:21]=1[Cl:26]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 22760614HCID 22760614, compound

Product 1

HCID 22760665HCID 22760665, compound

Procedure

8 g of 4-(4-chloro-3-o-chlorobenzylsulfamoylphenyl)-3-methyl-2-methylimino-1,3-thiazolidine-4-ol were reacted as prescribed in Example 3(c) with ethanolic HCl solution and the end product was precipitated by adding ethyl acetate. Colorless crystals, melting point: 170° C. (decomposition).

Workup

  1. customthe end product was precipitated
  2. additionby adding ethyl acetate

Sources & evidence

ORD record
ord-ef104e8305ce4b5184f173d09757392b
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

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