Hydrogen Bromide → HCID 22760637, compound

Participants

Reaction Steps

2.5 g of 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-cyclohexyl-2-cyclohexylimino-1,3-thiazolidine-4-ol were dissolved in 10 ml of methanol and adjusted to pH 3 by adding dropwise 48% hydrobromic acid. The solvent was distilled off under reduced pressure and the amorphous end product was crystallized under diethyl ether. Colorless crystals, melting point: 131° C. (decomposition).

Provenance & Evidence