HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22760497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 22760620 | HCID 22760620 | — |
| Solvent | Diglyme | HCID 8150 | — |
| Product | HCID 22760497 | HCID 22760497 | — |
Reaction Steps
18 g of the 3-di-n-butylsulfamoyl-4-chlorobenzoylchloride so obtained as an oil were reacted as prescribed in Example 70(c) in diethyl ether with diazomethane and then with concentrated HCl in diethyleneglycol dimethyl ether and worked up, 3'-di-n-butylsulfamoyl-2,4'-dichloroacetophenone being obtained in the form of colorless crystals having a melting point of 71° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125614 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-62ac71b2290247be8d02acdfc04c9965 |
| Source note | uspto-grants-1978_11 |