Hydrochloric Acid → HCID 22760497, compound

HRID 1703933Notes

Reaction equation

HRID 1703933 reaction equation
[CH2:1]([N:5]([CH2:19][CH2:20][CH2:21][CH3:22])[S:6]([C:9]1[CH:10]=[C:11]([CH:15]=[CH:16][C:17]=1[Cl:18])C(Cl)=O)(=[O:8])=[O:7])[CH2:2][CH2:3][CH3:4].[N+](=C)=[N-].[ClH:26].C([O:29][CH2:30][CH3:31])C>COCCOCCOC>[CH2:1]([N:5]([CH2:19][CH2:20][CH2:21][CH3:22])[S:6]([C:9]1[CH:10]=[C:11]([C:30](=[O:29])[CH2:31][Cl:26])[CH:15]=[CH:16][C:17]=1[Cl:18])(=[O:7])=[O:8])[CH2:2][CH2:3][CH3:4]

Participants

6

Reactant 4

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 9550DiazomethaneHCID 22760620HCID 22760620, compound

Product 1

HCID 22760497HCID 22760497, compound

Reagents, catalysts & solvents 1

HCID 8150DiglymeSolvent

Procedure

18 g of the 3-di-n-butylsulfamoyl-4-chlorobenzoylchloride so obtained as an oil were reacted as prescribed in Example 70(c) in diethyl ether with diazomethane and then with concentrated HCl in diethyleneglycol dimethyl ether and worked up, 3'-di-n-butylsulfamoyl-2,4'-dichloroacetophenone being obtained in the form of colorless crystals having a melting point of 71° C.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-62ac71b2290247be8d02acdfc04c9965
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

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