N,N'-Diethylthiourea → HCID 22760452, compound

HRID 1703934Notes

Reaction equation

HRID 1703934 reaction equation
[CH2:1]([N:5]([CH2:20][CH2:21][CH2:22][CH3:23])[S:6]([C:9]1[CH:10]=[C:11]([C:16](=[O:19])[CH2:17]Cl)[CH:12]=[CH:13][C:14]=1[Cl:15])(=[O:8])=[O:7])[CH2:2][CH2:3][CH3:4].[CH2:24]([NH:26][C:27]([NH:29][CH2:30][CH3:31])=[S:28])[CH3:25]>>[ClH:15].[CH2:30]([N:29]1[C:16]([C:11]2[CH:12]=[CH:13][C:14]([Cl:15])=[C:9]([S:6](=[O:8])(=[O:7])[N:5]([CH2:20][CH2:21][CH2:22][CH3:23])[CH2:1][CH2:2][CH2:3][CH3:4])[CH:10]=2)([OH:19])[CH2:17][S:28][C:27]1=[N:26][CH2:24][CH3:25])[CH3:31]

Participants

3

Reactant 2

HCID 2735009N,N'-DiethylthioureaHCID 22760497HCID 22760497, compound

Product 1

HCID 22760452HCID 22760452, compound

Procedure

7.0 g of 3'-di-n-butylsulfamoyl-2,4'-dichloro-acetophenone were reacted according to Example 12 with 2.7 g of 1,3-diethylthiourea and worked up. Colorless solid body, decomposition beginning at 139° C., γ C=N 1615 cm-1.

Workup

  1. customat 139° C.

Sources & evidence

ORD record
ord-135ea275b0f243a9844dadbaac415f33
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

Loading…