Hydrochloric Acid → HCID 67111990, compound
Reaction equation
[Si:1]([OH:5])([OH:4])([OH:3])[OH:2].[C:6]1([OH:12])[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1.[CH2:13]=[O:14].Cl>>[Si:1]([OH:5])([OH:4])([OH:3])[OH:2].[C:6]1([OH:12])[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1.[CH2:13]=[O:14]Participants
4
Procedure
The phenol silicate compound produced in Example 2 is added to an aqueous solution of formaldehyde in the ratio of 1 to 3 mols. A dilute mineral acid, hydrochloric acid, is added to the mixture until the pH is 5 to 6 then heated to 65° to 120° C. for 10 to 90 minutes while agitating at ambient pressure thereby producing poly (formaldehyde phenol silicate) resinous product.
Workup
- temperaturethen heated to 65° to 120° C. for 10 to 90 minutes
Sources & evidence
- ORD record
- ord-88bc00347cdd433690741a669be82d27
- Source dataset
- uspto-grants-1978_11
- Patent number
- US04125703
Reaction notes
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