Sodium Iodide → HCID 54034935, compound

HRID 1703970Notes

Reaction equation

HRID 1703970 reaction equation
[CH2:1]([C:3](=[CH:7][CH:8]=[CH:9][C:10]1[CH:15]=[CH:14][C:13]2[O:16][CH2:17][O:18][C:12]=2[CH:11]=1)[CH2:4][CH2:5]Br)[CH3:2].[I-:19].[Na+]>CC(C)=O>[CH2:1]([C:3](=[CH:7][CH:8]=[CH:9][C:10]1[CH:15]=[CH:14][C:13]2[O:16][CH2:17][O:18][C:12]=2[CH:11]=1)[CH2:4][CH2:5][I:19])[CH3:2]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 53884915HCID 53884915, compound

Product 1

HCID 54034935HCID 54034935, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

3-Ethyl-6-(3,4-methylenedioxyphenyl)-3,5-hexadienyl iodide [IX; Ar is 3,4-methylenedioxyphenyl, R is C2H5 ] was prepared from 10 g. of 3-ethyl-6-(3,4-methylenedioxyphenyl)-3,5-hexadienyl bromide (Preparation C9) and 6 g. of sodium iodide in 120 ml. of acetone, to give 10.5 g. of product as an oil.

Sources & evidence

ORD record
ord-1cf01080e2444daf82431bff0d3687c5
Source dataset
uspto-grants-1978_11
Patent number
US04125541

Reaction notes

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