HRID1704068

反应详情

EQUATION

反应方程式

HRID 1704068 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a suspension of 2.18 g of methyl α-(p-tert-butylphenoxy)-α-[p-(p-nitrophenoxy)phenyl]acetate in 50 ml of methanol was added 160 mg of 10% palladium on carbon and the mixture hydrogenated with shaking. The mixture was filtered and the filtrate concentrated under vacuum to give 2.1 g of the product as a gum.

WORKUP

后处理

  1. filtrationThe mixture was filtered
  2. concentrationthe filtrate concentrated under vacuum