HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12531881, compound → HCID 20392639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12531881 | HCID 12531881 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20392639 | HCID 20392639 | 103.5% |
Reaction Steps
To a suspension of 2.18 g of methyl α-(p-tert-butylphenoxy)-α-[p-(p-nitrophenoxy)phenyl]acetate in 50 ml of methanol was added 160 mg of 10% palladium on carbon and the mixture hydrogenated with shaking. The mixture was filtered and the filtrate concentrated under vacuum to give 2.1 g of the product as a gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125729 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-bcf180e2493240a0998393232332d070 |
| Source note | uspto-grants-1978_11 |