HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22761079, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-Chlorophenol | HCID 4684 | — |
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 10633141 | HCID 10633141 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22761079 | HCID 22761079 | 73.6% |
Reaction Steps
To a solution of 2.58 g of p-chlorophenol in 25 ml of ethanol is added 2.64 g of 85% potassium hydroxide solution, 3.6 g of potassium iodide and 4.6 g of [p-(3-chloropropoxy)phenyl]acetic acid. The mixture is refluxed for 18 hours, diluted with water, acidified with concentrated HCl and filtered to give 4.74 g of crystals. Recrystallization from acetic acid-water gives 3.85 g of white crystals, mp slowly melts 131°-150° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125732 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-4a5c5d5676af485191d594dd5304c42b |
| Source note | uspto-grants-1978_11 |