HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 54411517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | 3-(Trifluoromethyl)phenol | HCID 7376 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 22761172 | HCID 22761172 | — |
| Solvent | Hexamethylphosphoramide | HCID 12679 | — |
| Product | HCID 54411517 | HCID 54411517 | — |
Reaction Steps
As described in Example 30, a mixture of 3.4 g of m-trifluoromethylphenol, 0.755 g of 60% sodium hydride-oil dispersion, 3.5 g of potassium iodide, one ml of hexamethylphosphoramide and 7.9 g of methyl bromo{p-[3-(p-chlorophenoxy)propoxy]phenyl}acetate in 70 ml of tetrahydrofuran is refluxed for 18 hours and worked-up to give 10 g of oil. Purification gives 8.6 g of light amber oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125732 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-5d32361313ba4f86bd528e1e5bcb5c07 |
| Source note | uspto-grants-1978_11 |