3-Chlorophenol → HCID 131711340, compound

HRID 1704114Notes

Reaction equation

HRID 1704114 reaction equation
Br[CH:2]([C:7]1[CH:12]=[CH:11][C:10]([O:13][CH2:14][CH2:15][CH2:16][O:17][C:18]2[CH:23]=[CH:22][C:21]([Cl:24])=[CH:20][CH:19]=2)=[CH:9][CH:8]=1)[C:3]([O:5][CH3:6])=[O:4].[Cl:25][C:26]1[CH:27]=[C:28]([OH:32])[CH:29]=[CH:30][CH:31]=1>>[CH3:6][O:5][C:3](=[O:4])[CH:2]([O:32][C:28]1[CH:29]=[CH:30][CH:31]=[C:26]([Cl:25])[CH:27]=1)[C:7]1[CH:12]=[CH:11][C:10]([O:13][CH2:14][CH2:15][CH2:16][O:17][C:18]2[CH:23]=[CH:22][C:21]([Cl:24])=[CH:20][CH:19]=2)=[CH:9][CH:8]=1

Participants

3

Reactant 2

HCID 79333-ChlorophenolHCID 22761172HCID 22761172, compound

Product 1

HCID 131711340HCID 131711340, compoundYield 95.3%

Procedure

As described in Example 44, 8.28 g of methyl bromo{p-[3-(p-chlorophenoxy)propoxy]phenyl}acetate is reacted with 2.96 g of m-chlorophenol to give 8.8 g of the product as a viscous oil.

Sources & evidence

ORD record
ord-8c4ad6816c5c41a7877174d6ddb28beb
Source dataset
uspto-grants-1978_11
Patent number
US04125732

Reaction notes

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