4-Chlorophenol → HCID 54300003, compound

HRID 1704130Notes

Reaction equation

HRID 1704130 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][CH:3]=1.Br[CH:10]([C:15]1[CH:20]=[CH:19][C:18]([O:21][CH2:22][CH:23]([O:25][C:26]2[CH:31]=[CH:30][C:29]([Cl:32])=[CH:28][CH:27]=2)[CH3:24])=[CH:17][CH:16]=1)[C:11]([O:13][CH3:14])=[O:12]>>[CH3:14][O:13][C:11](=[O:12])[CH:10]([O:8][C:5]1[CH:6]=[CH:7][C:2]([Cl:1])=[CH:3][CH:4]=1)[C:15]1[CH:20]=[CH:19][C:18]([O:21][CH2:22][CH:23]([O:25][C:26]2[CH:31]=[CH:30][C:29]([Cl:32])=[CH:28][CH:27]=2)[CH3:24])=[CH:17][CH:16]=1

Participants

3

Reactant 2

HCID 46844-ChlorophenolHCID 53755495HCID 53755495, compound

Product 1

HCID 54300003HCID 54300003, compoundYield 79.4%

Procedure

As described in Example 71, 2.19 g of p-chlorophenol is reacted with 7.0 g of methyl bromo{p-[2-(p-chlorophenoxy)propoxy]phenyl}acetate to give 6.2 g of product as a gum.

Sources & evidence

ORD record
ord-d16aaad42bba498697dd74b9541723bb
Source dataset
uspto-grants-1978_11
Patent number
US04125732

Reaction notes

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