HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 22761125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 54300003 | HCID 54300003 | — |
| Product | HCID 22761125 | HCID 22761125 | 98.3% |
Reaction Steps
As described in Example 73, 6.2 g of methyl (p-chlorophenoxy){p-[2-(p-chlorophenoxy)propoxy]phenyl}acetate is hydrolyzed with 4 g of potassium hydroxide to give 5.91 g of gum. Crystallization from hexane-ether gives 4.73 g of off-white crystals. Recrystallization from chloroform-hexane gives white crystals, mp 146°-148° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125732 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-c457231252fe4ab89587ebc60fc90145 |
| Source note | uspto-grants-1978_11 |