HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22761163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 22761173 | HCID 22761173 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22761163 | HCID 22761163 | — |
Reaction Steps
As in Example 56, 5.1 g of 2-(p-tert-butylphenoxy)-1-propanol is reacted with 2.3 ml of methanesulfonyl chloride in 150 ml of dichloromethane in the presence of 8 ml of triethylamine. The product (7.4 g) is obtained as an amber-colored liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125732 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-f206427bf0c942aeb5aabeaf4a53c594 |
| Source note | uspto-grants-1978_11 |