Triethylamine → HCID 22761163, compound

HRID 1704134Notes

Reaction equation

HRID 1704134 reaction equation
[C:1]([C:5]1[CH:15]=[CH:14][C:8]([O:9][CH:10]([CH3:13])[CH2:11][OH:12])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].[CH3:16][S:17](Cl)(=[O:19])=[O:18].C(N(CC)CC)C>ClCCl>[CH3:16][S:17]([O:12][CH2:11][CH:10]([O:9][C:8]1[CH:14]=[CH:15][C:5]([C:1]([CH3:2])([CH3:4])[CH3:3])=[CH:6][CH:7]=1)[CH3:13])(=[O:19])=[O:18]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 31297Methanesulfonyl chlorideHCID 22761173HCID 22761173, compound

Product 1

HCID 22761163HCID 22761163, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

As in Example 56, 5.1 g of 2-(p-tert-butylphenoxy)-1-propanol is reacted with 2.3 ml of methanesulfonyl chloride in 150 ml of dichloromethane in the presence of 8 ml of triethylamine. The product (7.4 g) is obtained as an amber-colored liquid.

Sources & evidence

ORD record
ord-f206427bf0c942aeb5aabeaf4a53c594
Source dataset
uspto-grants-1978_11
Patent number
US04125732

Reaction notes

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