HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 20378389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 1-Propanol, 2-(4-fluorophenoxy)- | HCID 10464730 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20378389 | HCID 20378389 | — |
Reaction Steps
As described in Example 56, 7.7 g of 2-(p-fluorophenoxy)-1-propanol is reacted with 8.8 ml of methanesulfonyl chloride in 400 ml of dichloromethane in the presence of 12.5 ml of triethylamine. The product is obtained as a pale yellow liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125732 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-bd34f44521494b72b6ca31fea84e8c99 |
| Source note | uspto-grants-1978_11 |