3,4-Dimethylphenol → HCID 54423799, compound

HRID 1704154Notes

Reaction equation

HRID 1704154 reaction equation
Br[CH:2]([C:7]1[CH:12]=[CH:11][C:10]([O:13][CH2:14][CH2:15][O:16][C:17]2[CH:22]=[CH:21][C:20]([F:23])=[CH:19][CH:18]=2)=[CH:9][CH:8]=1)[C:3]([O:5][CH3:6])=[O:4].[CH3:24][C:25]1[CH:26]=[C:27]([OH:32])[CH:28]=[CH:29][C:30]=1[CH3:31]>O1CCCC1>[CH3:24][C:25]1[CH:26]=[C:27]([CH:28]=[CH:29][C:30]=1[CH3:31])[O:32][CH:2]([C:7]1[CH:12]=[CH:11][C:10]([O:13][CH2:14][CH2:15][O:16][C:17]2[CH:22]=[CH:21][C:20]([F:23])=[CH:19][CH:18]=2)=[CH:9][CH:8]=1)[C:3]([O:5][CH3:6])=[O:4]

Participants

4

Reactant 2

HCID 72493,4-DimethylphenolHCID 53773398HCID 53773398, compound

Product 1

HCID 54423799HCID 54423799, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

As described in Example 71, methyl bromo{p-[2-(p-fluorophenoxy)ethoxy]phenyl}acetate (0.017 mole) is reacted with 3,4-dimethylphenol (0.017 mole) in 75 ml of tetrahydrofuran at 80° C. for 18 hrs to give the product as a gum.

Sources & evidence

ORD record
ord-e5d1b4811e9d44a5b7e7297571820a8d
Source dataset
uspto-grants-1978_11
Patent number
US04125732

Reaction notes

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