Hydrazinecarboxylic acid, ethyl ester → HCID 178473578, compound

Participants

Reaction Conditions

Reaction Steps

2-Penyl-4-imidazolecarboxaldehyde (8.16 g) is dissolved in hot ethanol (200 ml). A hot solution of ethyl carbazate (5.52 g) in ethanol (50 ml) is added. A precipitate forms immediately and the mixture is heated and stirred for about 10 minutes. The mixture is then cooled to 0° C and the precipitate collected by filtration to yield the title product, m.p. 196°-200° C.

Provenance & Evidence