HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 54248458, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Sesamol | HCID 68289 | — |
| Reactant | HCID 54070391 | HCID 54070391 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54248458 | HCID 54248458 | 63% |
Reaction Steps
Operating as described in Example 8 (part B), from 3 g of 1,7-dichloro-1-fluoro-1-heptene, 2.14 g of 3,4-methylendioxyphenol, 0.69 g of NaH and 30 ml of N,N-dimethylformamide there were obtained 2.8 g of the product of the above-cited formula, a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04126623 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-861272eaded643ee97ba6dc99b8f9de2 |
| Source note | uspto-grants-1978_11 |