Benzyl mercaptan → HCID 54428342, compound

Participants

Reaction Steps

2.43 g of benzylmercaptan were mixed with 30 ml of N,N-dimethylformamide and then additioned with 0.7 g of NaH (55% in paraffin oil). Thereupon, at room temperature and under stirring, into this mixture were dripped 3 g of 1,5-dichloro-1-fluoro-pent-1-ene. The mixture was stirred for 5 hours at 25° C. After washing with water, extraction with ether, drying and evaporizing, there were obtained 3 g of raw product purified by chromatography in a column (cis-, trans- isomer mixture) and which had the following characteristics:

Provenance & Evidence