HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4-methoxy-6-methyl-1,3,5-triazine → HCID 22757974, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4-methoxy-6-methyl-1,3,5-triazine | HCID 15466 | — |
| Reactant | Thiophene-2-sulfonyl isocyanate | HCID 12875192 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 22757974 | HCID 22757974 | — |
Reaction Steps
To a suspension of 14.0 g of 2-amino-4-methoxy-6-methyl-1,3,5-triazine in 300 ml. of acetonitrile was added, dropwise, 19 g of thiophene-2-sulfonyl isocyanate. After stirring for six hours, the mixture was filtered to yield the desired solid product melting at 182°-184° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04127405 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-7e125f107e2246ee9b0b3200d133523b |
| Source note | uspto-grants-1978_11 |