Phenethylamine → HCID 20394052, compound

HRID 1704682Notes

Reaction equation

HRID 1704682 reaction equation
[CH3:1][N:2]([CH3:15])[CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:14]=[CH:13][C:10]([CH:11]=O)=[CH:9][CH:8]=1.[CH2:16]([NH2:24])[CH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>C1(C)C=CC=CC=1>[CH3:1][N:2]([CH3:15])[CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:14]=[CH:13][C:10]([CH:11]=[N:24][CH2:16][CH2:17][C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[CH:9][CH:8]=1

Participants

4

Reactant 2

HCID 1001PhenethylamineHCID 5469324-[3-(Dimethylamino)propoxy]benzaldehyde

Product 1

HCID 20394052HCID 20394052, compoundYield 91.2%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

4-(3-Dimethylaminopropoxy)benzaldehyde (30.0 g) is reacted with 18 g of phenethylamine in 150 ml of toluene as described under Example 1 to give 41 g of an oil; boiling point 184°-189° C./0.1-0.2 mm of Hg.

Sources & evidence

ORD record
ord-65b3c90c9c4d4d95adb410256bd4425e
Source dataset
uspto-grants-1978_11
Patent number
US04127606

Reaction notes

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