HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → (2,5-Dimethoxybenzyl)(triphenyl)phosphonium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 2-(Bromomethyl)-1,4-dimethoxybenzene | HCID 592021 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | (2,5-Dimethoxybenzyl)(triphenyl)phosphonium bromide | HCID 19605777 | — |
Reaction Steps
The 2,5-dimethoxybenzyl triphenylphosphonium bromide is prepared by refluxing a mixture of 2,5-dimethoxybenzyl bromide (12 g.) and triphenylphosphine (14.2.) in acetonitrile (200 ml.) for one hour and isolating the product by standard methods.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04206225 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-25c7103be80d4232a5667bfba9256227 |
| Source note | uspto-grants-1980_06 |