HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23456142, compound → HCID 136149070, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23456142 | HCID 23456142 | — |
| Reactant | 6-Hydrazinyl-5-methoxy-3-pyridinesulfonamide | HCID 23456147 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 136149070 | HCID 136149070 | — |
Reaction Steps
4-(1-Carboxyethoxy)-1,2-naphthoquinone (0.22 g, 9×10-4) and 2-hydrazino-3-methoxy-5-sulfamoylpyridine (0.2 g, 9×10-4 mole) were added to acetic acid (15 ml), along with 2 to 3 drops of concentrated hydrochloric acid. After stirring overnight, the resulting precipitate was collected by filtration, air dried, slurried twice with boiling acetic acid (5 ml) and isolated again by filtration; yield, 80 mg (20 percent).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04207104 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-beb787eea94a4651a7b2de578dbd4325 |
| Source note | uspto-grants-1980_06 |