HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 20335754, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Zapizolam | HCID 68832 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20335754 | HCID 20335754 | — |
Reaction Steps
This compound was obtained in an analogous manner to that given in Example 10a from 15 grams of 6-(o-chloro-phenyl)-8-chloro-4H-s-triazolo-(4,3-a)-pyrido-(2,3-f)-(1,4)-diazepine and 55 grams of dimethylamine in 500 ml. of ethanol by heating for 5 hours at 120° C. M.P. 240°-242° C. (from methanol); Yield 8.5 grams.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04207322 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-19f174103fb74780bc4ed039568de886 |
| Source note | uspto-grants-1980_06 |