HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 20335569, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 20335504 | HCID 20335504 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20335569 | HCID 20335569 | — |
Reaction Steps
A mixture of 1.04 g. of 10-fluoroimidazo[1,2-a:3,4-a']diquinolin-15-ium iodide, 3.0 ml. of morpholine and 40 ml. of dimethylformamide is heated at gentle reflux for 40 hours, treated with 1.5 g. of sodium iodide and evaporated at reduced pressure to give 10-(4-morpholinyl)imidazo[1,2-a:3,4-a']diquinolin-15-ium iodide; m.p. >300° C. after two crystallizations from aqueous methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04207320 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-2db63b528f0f47f7bed454c25fa9f69c |
| Source note | uspto-grants-1980_06 |