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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1706434Generated: October 30, 2026

Morpholine → HCID 20335569, compound

https://huagongshe.com/reaction/1706434

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMorpholineHCID 8083—
ReactantHCID 20335504HCID 20335504—
SolventDimethylformamideHCID 6228—
ProductHCID 20335569HCID 20335569—

Reaction Steps

A mixture of 1.04 g. of 10-fluoroimidazo[1,2-a:3,4-a']diquinolin-15-ium iodide, 3.0 ml. of morpholine and 40 ml. of dimethylformamide is heated at gentle reflux for 40 hours, treated with 1.5 g. of sodium iodide and evaporated at reduced pressure to give 10-(4-morpholinyl)imidazo[1,2-a:3,4-a']diquinolin-15-ium iodide; m.p. >300° C. after two crystallizations from aqueous methanol.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04207320
Source datasetuspto-grants-1980_06
ORD IDord-2db63b528f0f47f7bed454c25fa9f69c
Source noteuspto-grants-1980_06