Hydrochloric Acid → HCID 20335496, compound

HRID 1706443Notes

Reaction equation

HRID 1706443 reaction equation
[I-].[F:2][C:3]1[CH:12]=[CH:11][C:10]2[N+:9]3[CH:13]=[C:14]4[CH:23]=[CH:22][C:21]5[CH:20]=[C:19]([CH3:24])[CH:18]=[CH:17][C:16]=5[N:15]4[C:8]=3[CH:7]=[CH:6][C:5]=2[CH:4]=1.[ClH:25]>>[Cl-:25].[F:2][C:3]1[CH:12]=[CH:11][C:10]2[N+:9]3[CH:13]=[C:14]4[CH:23]=[CH:22][C:21]5[CH:20]=[C:19]([CH3:24])[CH:18]=[CH:17][C:16]=5[N:15]4[C:8]=3[CH:7]=[CH:6][C:5]=2[CH:4]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 20335456HCID 20335456, compound

Product 1

HCID 20335496HCID 20335496, compound

Procedure

A hot solution of 88 g. of 3-fluoro-10-methylimidazo[1,2-a:3,4-a']diquinolin-15-ium iodide in 6.4 l. of 6 N hydrochloric acid is cooled and the resulting precipitate of 3-fluoro-10-methylimidazo[1,2-a:3,4-a']diquinolin-15-ium chloride is collected by filtration, washed with 0.4 N hydrochloric acid, then with acetone, and dried; m.p. 345°-350° C. (dec.).

Workup

  1. filtrationthe resulting precipitate of 3-fluoro-10-methylimidazo[1,2-a:3,4-a']diquinolin-15-ium chloride is collected by filtration
  2. washwashed with 0.4 N hydrochloric acid
  3. dry with materialwith acetone, and dried

Sources & evidence

ORD record
ord-5db263af4c6a46dc9f624984da572e5d
Source dataset
uspto-grants-1980_06
Patent number
US04207320

Reaction notes

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