HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 57178653, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 4(5H)-Benzothiazolone, 6,7-dihydro- | HCID 19839124 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57178653 | HCID 57178653 | 86% |
Reaction Steps
6 g (0.039 mole) of the ketone obtained in step (d) are dissolved in 50 ml anhydrous ethanol and treated for 30 minutes with a gaseous methylamine stream. After evaporation to dryness, the residue is taken up into ether and filtered, to give 5.6 g (86%) of product, M.p. 233°-235° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04208420 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-b61f206962e54c0791738650f81f1812 |
| Source note | uspto-grants-1980_06 |