Sodium Iodide → HCID 12463847, compound

Participants

Reaction Steps

A mixture of 17.5 g. (0.065 m) of 4-(4-methoxybenzyl)-cyclohexylmethyl bromide, 11 g. (0.073 m) of sodium iodide and 100 ml. of acetone was heated under reflux for two hours. The solvent was removed, the residue partitioned between water and ether, and the ether layer dried and concentrated to give 19.8 g. of oil, used directly in the next reaction.

Provenance & Evidence