HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-2-thiopseudourea sulfate → 58579-77-4
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-2-thiopseudourea sulfate | HCID 75270 | — |
| Reactant | HCID 12204071 | HCID 12204071 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 58579-77-4 | HCID 135449336 | 10.7% |
Reaction Steps
A mixture of N-(2-amino-6-methylbenzyl)glycine ethyl ester (0.972 g, 0.00437 mole) and 2-methyl-2-thiopseudourea sulfate (0.609 g, 0.00219 mole) in absolute ethanol (15 ml) was stirred at reflux for 16 hours. Workup as in Example 2 gave the title compound (47 mg), identical (ir) with authentic material prepared according to the procedure of J. Med. Chem., 18, 224 (1975).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04208521 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-ec075479741b4ffa8c0b0f1969286900 |
| Source note | uspto-grants-1980_06 |