Diazomethane → HCID 86737062, compound

Participants

Reaction Steps

Into 0.2 g of 9,9;15,15-bis-(ethylenedioxy)-13-prostenoic acid, ethereal diazomethane solution is dropped until a pale yellow color just remains. The organic solution is washed several times with aqueous sodium acetate solution. The organic phase is dried over MgSO4 and the solvent distilled. As the residue, 9,9;15,15-bis-(ethylenedioxy)-13-prostenoic acid methyl ester is obtained.

Provenance & Evidence