HRID1706866

反应详情

EQUATION

反应方程式

HRID 1706866 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

15 g of piperonal (0.1 mole), and 14.3 g of 3-morpholinoacetone (0.1 mole) are mixed in an aqueous-alcoholic sodium hydroxide solution (300 cm3 of 10% NaOH and 30 cm3 of ethanol). The mixture is stirred for 4 hours and the product obtained is then filtered. The product is rinsed with water and recrystallised from ethanol.

WORKUP

后处理

  1. customthe product obtained
  2. filtrationis then filtered
  3. washThe product is rinsed with water
  4. customrecrystallised from ethanol