HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperonal → 1-(3,4-Methylenedioxyphenyl)-4-morpholino-1-butene-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperonal | HCID 8438 | — |
| Reactant | 1-(4-Morpholinyl)acetone | HCID 11029948 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 1-(3,4-Methylenedioxyphenyl)-4-morpholino-1-butene-3-one | HCID 47967 | — |
Reaction Steps
15 g of piperonal (0.1 mole), and 14.3 g of 3-morpholinoacetone (0.1 mole) are mixed in an aqueous-alcoholic sodium hydroxide solution (300 cm3 of 10% NaOH and 30 cm3 of ethanol). The mixture is stirred for 4 hours and the product obtained is then filtered. The product is rinsed with water and recrystallised from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04209517 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-a6230ee247bb4822ab01e7931917fcdd |
| Source note | uspto-grants-1980_06 |