HRID1706867

反应详情

EQUATION

反应方程式

HRID 1706867 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

27.5 g of the ketone (0.1 M) obtained in Example 1 is dissolved in 300 cm3 of methanol and an aqueous solution of KBH4 is added dropwise. The reaction mixture is left overnight and decomposed with water. The product obtained is filtered and recrystallised in ethanol.

WORKUP

后处理

  1. additionan aqueous solution of KBH4 is added dropwise
  2. customThe product obtained
  3. filtrationis filtered
  4. customrecrystallised in ethanol