HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1-(3,4-Methylenedioxyphenyl)-4-morpholino-1-butene-3-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1-(3,4-Methylenedioxyphenyl)-4-morpholino-1-butene-3-one | HCID 47967 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-(3,4-Methylenedioxyphenyl)-4-morpholino-1-butene-3-ol | HCID 47971 | — |
Reaction Steps
27.5 g of the ketone (0.1 M) obtained in Example 1 is dissolved in 300 cm3 of methanol and an aqueous solution of KBH4 is added dropwise. The reaction mixture is left overnight and decomposed with water. The product obtained is filtered and recrystallised in ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04209517 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-842c2a0ae5a34c11a258e3a737fab6a7 |
| Source note | uspto-grants-1980_06 |