Methanol → HCID 178517647, compound
Reaction equation
[F:1][C:2]1[CH:3]=[C:4]([C:8]([CH2:10]C=O)=N)[CH:5]=[CH:6][CH:7]=1.[NH2:13][C:14]([NH2:16])=[O:15].[CH3:17]O>>[F:1][C:2]1[CH:3]=[C:4]([C:8]2[CH:10]=[N:13][C:14]([OH:15])=[N:16][CH:17]=2)[CH:5]=[CH:6][CH:7]=1Participants
4
Procedure
By the procedure described in Example 4, (m-fluorophenyl)formimidoylacetaldehyde is reacted with urea to give the product of the Example (recrystallized from methanol), m.p. 259°-261° C.
Workup
- customto give
Sources & evidence
- ORD record
- ord-5ab3f261b4a14700b4d00313898058f6
- Source dataset
- uspto-grants-1980_06
- Patent number
- US04209621
Reaction notes
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