HuagongsheHuagongshe Chemistry Print Report · For research reference only
Magnesium orthosilicate → HCID 1478870, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Magnesium orthosilicate | HCID 66225 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | o-Fluoroacetophenone | HCID 96744 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 1478870 | HCID 1478870 | — |
Reaction Steps
A mixture of 25.0 g. of o-fluoroacetophenone and 35 ml. of dimethylformamide dimethylacetal is refluxed for 16 hours. Evaporation gives a thick oil which is dissolved in methylene chloride and passed through a short column of hydrous magnesium silicate. Evaporation of the solvent gives 34.2 g. of the desired compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04209621 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-3c095e3aabc94467adbbb5b2c391bfa5 |
| Source note | uspto-grants-1980_06 |