HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-5-methyl-4H-1,2,4-triazole → HCID 20333328, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-5-methyl-4H-1,2,4-triazole | HCID 234610 | — |
| Reactant | 3-Dimethylamino-3'-trifluoromethylacrylophenone | HCID 730024 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20333328 | HCID 20333328 | — |
Reaction Steps
A mixture of 0.49 g. of 3-amino-5-methyl-1,2,4-triazole and 1.26 g. of 3-dimethylamino-3'-trifluoromethylacrylophenone in 25 ml. of glacial acetic acid refluxed for 16 hours. The resulting mixture is worked up as described in Example 54 to give the product of the Example, m.p. 153°-154° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04209621 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-a6cebb3b2f984f8e9e9bc8a3894c4380 |
| Source note | uspto-grants-1980_06 |