HRID1707062

反应详情

EQUATION

反应方程式

HRID 1707062 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 2.24 g. of 3-amino-5-ethyl-1,2,4-triazole and 4.86 g. of 3-dimethylamino-3'-trifluoromethylacrylophenone in 50 ml. of glacial acetic acid is refluxed for 16 hours. The resulting mixture is worked up as described in Example 54 to give the product of the Example, m.p. 132°-134° C.

WORKUP

后处理

  1. additionA mixture of 2.24 g
  2. customto give the product of the Example, m.p. 132°-134° C.