HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Dimethylamino)-1-[2-(trifluoromethyl)phenyl]prop-2-en-1-one → HCID 20333363, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Dimethylamino)-1-[2-(trifluoromethyl)phenyl]prop-2-en-1-one | HCID 54259832 | — |
| Reactant | HCID 178418311 | HCID 178418311 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20333363 | HCID 20333363 | — |
Reaction Steps
A mixture of 1.68 g. of 3-amino-1,2,4-triazole and 4.86 g. of 3-dimethylamino-2'-trifluoromethylacrylophenone in 25 ml. of glacial acetic acid refluxed for 16 hours. The resulting mixture is worked up as described in Example 54 to yield the product of the Example, m.p. 149°-151° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04209621 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-446dce4980d1430f82490e44e3e0eb0a |
| Source note | uspto-grants-1980_06 |