HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Dimethylamino)-1-phenyl-2-propen-1-one → HCID 178527861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Dimethylamino)-1-phenyl-2-propen-1-one | HCID 353460 | — |
| Reactant | Thiourea | HCID 2723790 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178527861 | HCID 178527861 | — |
Reaction Steps
A mixture of 17.5 g. of 3-dimethylaminoacrylophenone and 30.44 g. of thiourea is intimately mixed and fused at 180°-190° C. for one hour. The mixture is cooled and water is added and the desired compound is recovered by filtration, m.p. 203°-205° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04209621 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-b24124d418164577b413617eda53f90f |
| Source note | uspto-grants-1980_06 |