HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 20333327, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178506145 | HCID 178506145 | — |
| Product | HCID 20333327 | HCID 20333327 | — |
Reaction Steps
A solution of 4.75 g. of 2-mercapto-4-(m-trifluoromethylphenyl)pyrimidine in 50 ml. of 1 N sodium hydroxide is cooled to near 0° C. in an ice bath and 2.90 g. of methyliodide is added. After the reaction mixture is allowed to warm to room temperature, the product is removed by filtration, m.p. 89°-90° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04209621 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-98a3e24346a743f692a31882b67163be |
| Source note | uspto-grants-1980_06 |