HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chlorophenyl)-2-hydrazinopyridine → HCID 20333397, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chlorophenyl)-2-hydrazinopyridine | HCID 20300092 | — |
| Reactant | Ethylorthoformate | HCID 53630039 | — |
| Product | HCID 20333397 | HCID 20333397 | — |
Reaction Steps
A mixture of 8.5 g. of 5-(4-chlorophenyl)-2-hydrazinopyridine and 80.0 ml. of ethyl orthoformate is refluxed for 5 hours. The mixture is filtered and the solid is washed with hexane to give 6.5 g. of the product of the Example, m.p. 259°-262° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04209626 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-ae12a02c2f8d48fd94c9e19c4b51b320 |
| Source note | uspto-grants-1980_06 |