2-Aminopyrimidine → HCID 86748162, compound

Participants

Reaction Steps

(S)-Lactic acid (3.0 g; 28 mmol) was dissolved in methanol (5 cm3) and added to a solution of 2-aminopyrimidine (2.7 g; 28 mmol) in methanol (5 cm3). The resulting white product was collected by filtration, recrystallized from water, and dried in vacuo. Found: C, 58.0%; H, 5.4%; N, 16.8%. Calculated for C12H13N3O3 : C, 58.28%; N, 5.31%; N, 17.00%. M.pt. 125°-127° C.

Provenance & Evidence